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L-Lysine monohydrochloride or L-Lysine hydrochloride or L-Lysine HCl USP BP Ph Eur FCC Food Grade Manufacturers
Anmol Chemicals is a manufacturer supplier exporter of L-Lysine monohydrochloride or L-Lysine hydrochloride or L-Lysine HCl and it offers materials as per IP BP EP Ph Eur USP NF JP FCC Food Grade as per the the latest monograph at best prices. Anmol Chemicals Group, established in 1976, is the pioneer manufacturer of Specialty Chemicals, Pharmaceutical Excipients, Some API, Food Chemicals in India. Anmol Chemicals Group has manufacturing facilities spread across Western India, representatives in Houston, Chicago USA and Dubai, UAE. We also have toll manufacturing units for processing chemicals in a few countries around the world. We make IP, BP, EP, USP, NF, Ph. Eur., JP, FCC or Food Grade, Analytical Reagent Grade, LR or Laboratory Reagent Grades and Pure Grades of various chemicals. All our items are analyzed to meet the required standards. We can supply the product in grams for your laboratory trial and in tons for your plant scale jobs.
We manufacture Bulk Drugs / API, Excipients, Pharmaceuticals (IP BP USP NF Ph Eur EP JP), Specialty Chemicals (Pure/Reagent), Mineral Fortifiers (FCC). Our manufacturing facility is FDA approved and GLP, cGMP, ISO9001, ISO14001, ISO/IEC 17025, ISO22000, FSSC 22000, ISO45001, FSSAI, Kosher, HALAL, COPP, WHO-GMP certified and Written Confirmation (WC) is available. Solid materials can be customized for particle size, shape, and bulk density. We observe WHO Good Manufacturing Practices and Good Laboratory Practices. We are a government-recognized STAR Export House and "Authorised Economic Operator (AEO)" per Indian Customs.
All technical documents and DMF support available.
L-Lysine monohydrochloride or L-Lysine hydrochloride or L-Lysine HCl SDS of Manufacturers
Synonyms: L-Lysine monohydrochloride or Lysine Hydrochloride or 2,6-Diaminohexanoic acid monohydrochloride or 2,6-Diaminohexanoic Acid Hydrochloride
CAS Number: 657-27-2, Molecular Weight: 182.65, Chemical Formula: C6H14N2O2-HCl or H2N(CH2)4CH(NH2)CO2H-HCl, EINECS EC Number: 211-519-9, FEMA: ----,
Lysine Hydrochloride USP Grade
C6H14N2O2-HCl --- 182.65
Lysine Hydrochloride contains not less than 98.5 percent and not more than 101.5 percent of C6H14N2O2.HCl, as L-lysine hydrochloride, calculated on the dried basis.
Packaging and storage: Preserve in well-closed containers.
Identification: Infrared Absorption.
Specific rotation: between +20.4 and +21.4 .
Loss on drying: Dry it at 105C for 3 hours: it loses not more than 0.4% of its weight.
Residue on ignition: not more than 0.1%.
Sulfate: A solution containing 0.33 g shows no more sulfate than corresponds to 0.10 mL of 0.020 N sulfuric acid (0.03%).
Iron: 0.003%.
Heavy metals: 0.0015%.
Chromatographic purity: To pass the test.
Content of chloride: Transfer about 350 mg, accurately weighed, to a porcelain casserole, and add 140 mL of water and 1 mL of dichlorofluorescein. Mix, and titrate with 0.1 N silver nitrate until the silver chloride flocculates and the mixture acquires a faint pink color. Each mL of 0.1 N silver nitrate is equivalent to 3.545 mg of chloride: between 19.0% and 19.6% is found.
Assay: Transfer about 90 mg of Lysine Hydrochloride, accurately weighed, to a 125-mL flask, and dissolve in a mixture of 3 mL of formic acid and 50 mL of glacial acetic acid. Add 10 mL of mercuric acetate and titrate with 0.1 N perchloric acid, determining the endpoint potentiometrically. Perform a blank determination, and make any necessary correction. Each mL of 0.1 N perchloric acid is equivalent to 9.133 mg of C6H14N2O2.HCl.
Lysine Hydrochloride BP Ph Eur Grade
C6H14N2O2-HCl --- 182.7 --- CAS 657-27-2
Action and use: Amino acid.
DEFINITION
Lysine hydrochloride contains not less than 98.5 per cent and not more than the equivalent of 101.0 per cent of (S)-2,6-diaminohexanoic acid hydrochloride, calculated with reference to the dried substance.
CHARACTERS
A white or almost white, crystalline powder or colourless crystals, freely soluble in water, slightly soluble in alcohol.
IDENTIFICATION
First identification: A, B, E.
Second identification: A, C, D, E.
A. It complies with the test for specific optical rotation.
B. Examine by infrared absorption spectrophotometry, comparing with the spectrum obtained with lysine hydrochloride CRS. Examine the substances prepared as discs. If the spectra obtained show differences, dissolve the substance to be examined and the reference substance separately in the minimum volume of water, evaporate to dryness at 60C, and record new spectra using the residues.
C. Examine the chromatograms obtained in the test for ninhydrin-positive substances. The principal spot in the chromatogram obtained with test solution (b) is similar in position, colour and size to the principal spot in the chromatogram obtained with reference solution (a).
D. To 0.1 ml of solution S (see Tests) add 2 ml of water and 1 ml of a 50 g/l solution of phosphomolybdic acid. A yellowish-white precipitate is formed.
E. To 0.1 ml of solution S add 2 ml of water. The solution gives reaction (a) of chlorides.
TESTS
Solution S: Dissolve 5.0 g in carbon dioxide-free water R prepared from distilled water and dilute to 50 ml with the same solvent.
Appearance of solution: Solution S is clear and not more intensely coloured than reference solution.
Specific optical rotation: Dissolve 2.00 g in hydrochloric acid and dilute to 25.0 ml with the same acid. The specific optical rotation is + 21.0 to + 22.5, calculated with reference to the dried substance.
Ninhydrin-positive substances: To pass the test.
Sulphates: Dilute 5 ml of solution S to 15 ml with distilled water R. The solution complies with the limit test for sulphates (300 ppm).
Ammonium: 50 mg complies with limit test B for ammonium (200 ppm). Prepare the standard using 0.1 ml of ammonium standard solution (100 ppm NH4).
Iron: In a separating funnel, dissolve 0.33 g in 10 ml of dilute hydrochloric acid. Shake with three quantities, each of 10 ml, of methyl isobutyl ketone, shaking for 3 min each time. To the combined organic layers add 10 ml of water and shake for 3 min. The aqueous layer complies with the limit test for iron (30 ppm).
Heavy metals: 12 ml of solution S complies with limit test A for heavy metals (10 ppm).
Loss on drying: Not more than 0.5 per cent, determined on 1.000 g by drying in an oven at 105C.
Sulphated ash: Not more than 0.1 per cent, determined on 1.0 g.
ASSAY
Dissolve 0.150 g in 5 ml of anhydrous formic acid. Add 50 ml of anhydrous acetic acid. Titrate with 0.1 M perchloric acid, determining the end-point potentiometrically. 1 ml of 0.1 M perchloric acid is equivalent to 18.27 mg of C6H15ClN2O2.
STORAGE
Store protected from light.
L-Lysine Monohydrochloride FCC Food Grade
2,6-Diaminohexanoic Acid Hydrochloride
C6H14N2O2-HCl --- Formula wt 182.65 --- CAS: [657-27-2]
DESCRIPTION
L-Lysine Monohydrochloride occurs as a white or nearly white, free-flowing, crystalline powder. It is freely soluble in water, but it is almost insoluble in alcohol and in ether. It melts at about 260° with decomposition.
Function: Nutrient.
Identification: The infrared absorption spectrum of the sample exhibits relative maxima at the same wavelengths as those of a typical spectrum as shown in the section on Infrare-Spectra, using the same test conditions as specified therein.
Assay: Not less than 98.5% and not more than 101.5% of C6H14N2O2-HCl, calculated on the dried basis.
Lead: Not more than 5 mg/kg.
Loss on Drying: Not more than 1.0%.
Optical (Specific) Rotation: D20°: Between +20.3° and +21.5°, calculated on the dried basis; or D25°: Between +20.4° and +21.4°, calculated on the dried basis.
Residue on Ignition: Not more than 0.2%.
Keywords: L-Lysine monohydrochloride or Lysine Hydrochloride or 2,6-Diaminohexanoic acid monohydrochloride or 2,6-Diaminohexanoic Acid Hydrochloride IP BP Ph Eur EP USP Analytical Reagent FCC Food Grade CAS Number 657-27-2 Manufacturer Supplier Exporter Monograph Uses Chemical Molecular Formula Weight.
Manufacturer Supplier Exporter
ANMOL CHEMICALS
Now maturing as Anmol Chemicals Private Limited
Representatives in Houston, Chicago and New York, USA
TEL: (OFF) +91 22 23726950, +91 22 23774610, +91 22 23723564
Taloja Navi Mumbai, INDIA
e-mail: info@anmol.org
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Last updated
24-jun-24
Exporters to USA, Canada, UAE, Kuwait, Qatar, Gautemala, Tunisia, Europe, South Africa, Bangladesh, Sri Lanka, Tanzania, Kenya, Egypt, Iraq, Turkey, Israel, Vietnam, Nigeria, Uganda, Brazil, Chile, Argentina, Dubai, UAE, Saudi Arabia, Cameroon, Mexico, Brazil, Chile, Argentina, Korea, Thailand, Malaysia, Indonesia, Jakarta, Australia, China, Germany, France, etc.
Representatives in New York, Houston - Texas, Chicago - Illinois, Los Angeles.
All products are Sold for Industrial and Laboratory Use only. No other use is permitted.
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L-Lysine Hydrochloride
L-Lysine monohydrochloride or 2,6-Diaminohexanoic acid monohydrochloride or 2,6-Diaminohexanoic Acid Hydrochloride BP Ph Eur USP FCC Food Grades Manufacturers